HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetyl chloride → GS 389
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetyl chloride | HCID 7679 | — |
| Reactant | 1-Benzyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline | HCID 30024 | — |
| Reactant | 4-Methoxyphenylacetyl chloride | HCID 2734688 | — |
| Product | GS 389 | HCID 170524 | — |
Reaction Steps
1,2,3,4-Tetrahydro-1-(4-methoxybenzyl)-6,7-dimethoxyisoquinoline was prepared by a procedure analogous to that described in example 17 for 1,2,3,4-tetrahydro-1-benzyl-6,7-di-methoxyisoquinoline but substituting in the first step (4-methoxyphenyl)acetyl chloride for phenylacetyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981521 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-8fb7878d5365422c956cfe5e043fa3a3 |
| Source note | uspto-grants-1999_11 |