1-Bromopentane → HCID 19610702, compound
Reaction equation
[CH3:1][O:2][C:3]1([O:11][CH3:12])[CH:8]2[CH2:9][CH2:10][N:5]([CH2:6][CH2:7]2)[CH2:4]1.[Br:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]>>[Br-:13].[CH3:1][O:2][C:3]1([O:11][CH3:12])[CH:8]2[CH2:7][CH2:6][N+:5]([CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])([CH2:10][CH2:9]2)[CH2:4]1Participants
3
Conditions
- Temperature
- 110 °C
Procedure
A mixture of 3,3-dimethoxyquinuclidine (1.71 g, 10 mmol) and 1-bromopentane (1.51g, 10 mmol) was heated at 110° C. for 15 min. Yield 3.22 g, 100%.
Sources & evidence
- ORD record
- ord-ac7e27bdaabd4aafa897f1f08875e246
- Source dataset
- uspto-grants-1999_11
- Patent number
- US05981539
Reaction notes
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