6-Nitroveratraldehyde → HCID 53811859, compound

Participants

Reaction Steps

Prepared from 6-chloro-2-tetralone and 2-nitro-4,5-dimethoxybenzaldehyde; mp 56-58° C.; IR (Nujol): 2922, 1730, 1100; 1H NMR: δ2.68 (2H, t), 3.05 (2H t), 3.62 (3H, s), 3.98 (3H, s), 6.48 (1H, s), 6.82 (1H, d, J=8.4), 6.90-6.96 (1H, dd, J=8.4, 2.1), 7.26 (1H, d, J=2.1), 7.74 (1H, s), 8.01 (1H, s); 13C NMR: δ28.2, 37.4, 56.8, 56.9, 108.3, 112.2, 127.0, 127.2, 128.6, 130.9, 131.1, 133.3, 134.2, 134.5, 140.5, 141.5, 149.6, 153.7.

Provenance & Evidence