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HRID1602201

反应详情

EQUATION

反应方程式

HRID 1602201 的结构方程式

REACTANTS

反应物

2
结构：COc1cc(C=O)c([N+](=O)[O-])cc1OC
HCID88505

6-Nitroveratraldehyde

C9H9NO5

结构：O=C1CCc2ccc([N+](=O)[O-])cc2C1
HCID11321443

7-Nitro-2-tetralone

C10H9NO3

PRODUCTS

生成物

1
结构：COc1cc(C=C2C(=O)CCc3ccc([N+](=O)[O-])cc32)c([N+](=O)[O-])cc1OC
HCID54077917

未命名化合物

PROCEDURE

实验过程

Prepared from 7-nitro-2-tetralone and 2-nitro-4,5-dimethoxybenzaldehyde; mp 125° C.; IR (Nujol): 1724, 1540, 1545; 1H NMR: δ2.69 (2H, t), 3.16 (2H t), 3.59 (3H, s), 4.01 (3H, s), 6.45 (1H, s), 7.41 (1H, d, J=8.1), 7.68 (1H, d, J=2.2), 7.72 (1H, s), 7.94-7.99 (1H, dd, J=8.4, 2.2), 8.08 (1H, s); 13C NMR: δ28.4, 36.9, 56.9, 57.0, 108.7, 111.6, 123.2, 124.2, 126.1, 129.7, 132.5, 133.9, 135.8, 141.4, 145.8, 146.8, 150.1, 154.1, 198.4.