HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxybenzylamine → HCID 19610565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxybenzylamine | HCID 21156 | — |
| Reactant | 2-(Bis(methylsulfanyl)methylidene)propanedinitrile | HCID 99229 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 19610565 | HCID 19610565 | — |
Reaction Steps
A mixture of 17.03 g (0.1 mol) of 3,3-bis-methylmercapto-2-cyano-acrylonitrile, 12.78 ml (0.1 mol) of 3-methoxy-benzylamine and 60 ml of ethyl acetate is heated under reflux for 2 hours and then concentrated by evaporation in vacuo, yielding the oily title compound; TLC-Rf 32 0.28 (toluene/isopropanol [9:1]).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981533 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-79761ac7d4a842049f9128fcf0ed5b93 |
| Source note | uspto-grants-1999_11 |