HCID 19611661, compound → HCID 19611702, compound

Participants

Reaction Steps

A solution of N-[3-(7-chloro-benzofuran-4-yl)-propyl]-acetamide (48 mg) in ethanol (15 ml) was hydrogenated over rhodium catalyst (5% on carbon; 15 mg) over 7 h. The catalyst was filtered off and the filtrate evaporated. The residue was purified by column chromatography, eluting with dichloromethane/methanol 50:1 gave the title compound as a colourless solid (37.6 mg) mp 76-78°

Provenance & Evidence