HCID 19611702, compound → HCID 10198333, compound

Participants

Reaction Steps

A solution of the N-[3-(7-chloro-2,3-dihydro-benzofuran-4-yl)-propyl]-acetamide, (78 mg) in ethanol (5 ml) was hydrogenated over palladium (10%; 20 mg) over 64 h. The catalyst was filtered off and the filtrate concentrated in vacuo. The residue was purified by column chromatography, eluting with dichloromethane/methanol 50:1 gave the title compound as a colourless solid (54 mg) mp 66-67° C.

Provenance & Evidence