HCID 19611639, compound → HCID 19611689, compound

Participants

Reaction Steps

A solution of N-[3-(5-chloro-benzofuran-4-yl)-propyl]-acetamide (0.25 g) in ethanol (15 ml) was hydrogenated over 5% rhodium on carbon (80 mg) for 18 h. The catalyst was filtered off and the filtrate evaporated. The residue was purified by column chromatography on silica, eluting with dichloromethane/methanol 40:1 gave the title compound as a colourless solid (131 mg) mp 91-92

Provenance & Evidence