HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2,3-dihydrobenzofuran-7-carboxylate → (2,3-Dihydro-1-benzofuran-7-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2,3-dihydrobenzofuran-7-carboxylate | HCID 15062252 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | (2,3-Dihydro-1-benzofuran-7-yl)methanol | HCID 2795020 | 80% |
Reaction Steps
Methyl 2,3-dihydro-benzofuran-7-carboxylate (12 g, 68 mmol) was reduced with LAH (5.14 g, 136 mmol) in THF similar to the above procedures to give the product as a dark oil (8.13 g, 80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981571 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-8baec61294a14182964f5fdf45b51e2a |
| Source note | uspto-grants-1999_11 |