HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 53961229, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | HCID 86754777 | HCID 86754777 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 53961229 | HCID 53961229 | — |
Reaction Steps
A solution of 2-4 (1.1 g, 3.9 mmol), p-TSA (5 mg) and acetone (50 mL) was heated at reflux for 1 hr. The cooled reaction mixture was diluted with EtOAc and then washed with sat. NaHCO3 and brine, dried (MgSO4), and concentration to afford 2-5 as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05981546 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-e70ead4d1f9b4d6e8e9a349a68ad71b6 |
| Source note | uspto-grants-1999_11 |