Sodium Hydroxide → HCID 22086393, compound

Participants

Reaction Steps

To a solution 13-8 (527 mg, 1.75 mmol) in EtOH was added 1N NaOH (1.93 mL, 1.925 mmol). After stirring for 1 h, the solvents were evaporated, the mixture was diluted with EtOAc, acidified with 10% KHSO4, washed with brine, dried over MgSO4, and evaporated to give 13-9 as a white solid.

Provenance & Evidence