HRID1602665

反应详情

EQUATION

反应方程式

HRID 1602665 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

##STR54## To a degassed solution of the pyridone 16-5 (243 mg; 0.49 mmol) in EtOH (20 mL) was added 10% Pd on carbon (25 mg) and this was then stirred under an atmosphere of hydrogen gas (balloon) for 3 hours. The mixture was filtered through a pad of celite and the solvent removed to give the title compound (16-6) as a viscous oil which was used as such in the next step.

WORKUP

后处理

  1. filtrationThe mixture was filtered through a pad of celite
  2. customthe solvent removed