HRID1602903
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of 6-hydroxymethyl-5-(2-methoxymethoxy-4-methoxyphenyl)4-propoxy-pyrimidine in CH2Cl2 was treated with MnO2 and stirred vigorously for 24 h. The mixture was filtered through celite and concentrated to afford the tide compound (1.48 g, 62%).
WORKUP
后处理
- filtrationThe mixture was filtered through celite
- concentrationconcentrated