HRID1602903

反应详情

EQUATION

反应方程式

HRID 1602903 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 6-hydroxymethyl-5-(2-methoxymethoxy-4-methoxyphenyl)4-propoxy-pyrimidine in CH2Cl2 was treated with MnO2 and stirred vigorously for 24 h. The mixture was filtered through celite and concentrated to afford the tide compound (1.48 g, 62%).

WORKUP

后处理

  1. filtrationThe mixture was filtered through celite
  2. concentrationconcentrated