Sodium Hydroxide → HCID 53864972, compound

HRID 1602945Notes

Reaction equation

HRID 1602945 reaction equation
[CH2:1]([C:5]1[N:6]([CH2:16][C:17]2[CH:22]=[CH:21][C:20]([C:23]3[C:24]([C:29]([O:31]C)=[O:30])=[CH:25][CH:26]=[CH:27][CH:28]=3)=[CH:19][CH:18]=2)[C:7]2[C:12]([C:13](=[O:15])[CH:14]=1)=[CH:11][CH:10]=[CH:9][CH:8]=2)[CH2:2][CH2:3][CH3:4].[OH-].[Na+]>C(O)C>[CH2:1]([C:5]1[N:6]([CH2:16][C:17]2[CH:18]=[CH:19][C:20]([C:23]3[C:24]([C:29]([OH:31])=[O:30])=[CH:25][CH:26]=[CH:27][CH:28]=3)=[CH:21][CH:22]=2)[C:7]2[C:12]([C:13](=[O:15])[CH:14]=1)=[CH:11][CH:10]=[CH:9][CH:8]=2)[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 19608485HCID 19608485, compound

Product 1

HCID 53864972HCID 53864972, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Using the procedure of Example 2, the product of Example 19 and 3 ml of N sodium hydroxide and 2 ml of ethanol were reacted to obtain after crystallization from dimethylformamide, 155 mg of the desired product melting at >260° C.

Workup

  1. customto obtain
  2. customafter crystallization from dimethylformamide, 155 mg of the desired product melting at >260° C.

Sources & evidence

ORD record
ord-8b7de2e9e77b4484aa4d74e0e7de08c1
Source dataset
uspto-grants-1999_11
Patent number
US05985894

Reaction notes

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