HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-tert-Butylcatechol → HCID 15289112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-tert-Butylcatechol | HCID 7381 | — |
| Reactant | Maleimide | HCID 10935 | — |
| Reactant | 1,3-Cyclohexadiene-1-carboxylic acid, ethyl ester | HCID 11094816 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15289112 | HCID 15289112 | — |
Reaction Steps
13.5 g (0.138 mol) of maleimide and 25.3 g (0.17 mol) of ethyl 1,3-cyclohexadiene-1-carboxylate are heated under reflux with 1.4 g of 4-(tert-butyl)pyrocatechol in 275 ml of toluene overnight. The mixture is concentrated and the residue is recrystallized from isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05986105 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-1cf43784c2d54a018950786a8b405149 |
| Source note | uspto-grants-1999_11 |