HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15289119, compound → HCID 15289108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15289119 | HCID 15289119 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 15289108 | HCID 15289108 | — |
Reaction Steps
45 g (0.234 mol) of 1-amino-4-azatricyclo[5.2.2.02,6 ]undec-8-ene-3,5-dione are reduced with 24 g of LiAlH4 in 500 ml of absolute dioxane as under Z 1-B and the mixture is worked up accordingly.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05986105 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-f638046841d54dbbbf52ea294348e49e |
| Source note | uspto-grants-1999_11 |