HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1603667Generated: November 1, 2026
1-Chloro-3-iodobenzene → HCID 19605228, compound
https://huagongshe.com/reaction/1603667
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Chloro-3-iodobenzene | HCID 12269 | — |
| Reactant | 5-Hexyn-1-ol | HCID 70234 | — |
| Catalyst | Tetrakis(triphenylphosphine)palladium | HCID 11979704 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 19605228 | HCID 19605228 | — |
Reaction Steps
A mixture of 3-chloroiodobenzene (14.3 g, 60 mmol), tetrakis(triphenylphosphine) palladium (2.1 g, 1.8 mmol) and 5-hexyn-1-ol (5.9 g, 60 mmol) in triethylamine (120 ml) was stirred at 25° C. for 3H and partitioned between water and ether. The
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05990102 |
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| Source dataset | uspto-grants-1999_11 |
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| ORD ID | ord-85ba4a580d8f4dc287c23dc6ed4c11d6 |
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| Source note | uspto-grants-1999_11 |
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