HCID 15289116, compound → HCID 15289117, compound

HRID 1603693Notes

Reaction equation

HRID 1603693 reaction equation
[C:1]([C:3]12[CH2:13][CH2:12][CH:9]([CH:10]=[CH:11]1)[CH:8]1[CH:4]2[C:5](=O)[NH:6][C:7]1=O)#[N:2].[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[NH2:2][CH2:1][C:3]12[CH2:13][CH2:12][CH:9]([CH:10]=[CH:11]1)[CH:8]1[CH:4]2[CH2:5][NH:6][CH2:7]1

Participants

3

Reactant 2

HCID 15289116HCID 15289116, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 15289117HCID 15289117, compound

Procedure

15.4 g (76.2 mmol) of 1-cyano-4-azatricyclo[5.2.2.02,6 ]undec-8-ene-3,5-dione are reduced with LiAlH4 as described under Z 1-B and the mixture is worked up accordingly.

Sources & evidence

ORD record
ord-d441b9a0ed954538b6dac566515b45b6
Source dataset
uspto-grants-1999_11
Patent number
US05990122

Reaction notes

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