HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15289121, compound → HCID 15289122, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15289121 | HCID 15289121 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15289122 | HCID 15289122 | — |
Reaction Steps
7.4 g (27.5 mmol) of 1-aminomethyl-4-benzyl-4-azatricyclo[5.2.2.02,6 ]undec-8-ene are hydrogenated in 100 ml of tetrahydrofuran using 1.5 g of palladium/active charcoal at 100° C./100 bar. The catalyst is filtered off with suction and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990122 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-80dfa729c0d74ca897188dc7c94d27ed |
| Source note | uspto-grants-1999_11 |