2-Imidazolidinone, 1-(p-chlorophenyl)- → HCID 86754836, compound

HRID 1603749Notes

Reaction equation

HRID 1603749 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:12][CH2:11][NH:10][C:9]2=[O:13])=[CH:4][CH:3]=1.Cl[CH2:15][CH2:16][CH2:17][O:18][C:19]1[CH:26]=[CH:25][C:22]([CH:23]=[O:24])=[CH:21][CH:20]=1.ClCCOC1C=CC(C=O)=CC=1>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([N:8]2[CH2:12][CH2:11][N:10]([CH2:15][CH2:16][CH2:17][O:18][C:19]3[CH:26]=[CH:25][C:22]([CH:23]=[O:24])=[CH:21][CH:20]=3)[C:9]2=[O:13])=[CH:6][CH:7]=1

Participants

4

Reactant 3

HCID 264512-Imidazolidinone, 1-(p-chlorophenyl)-HCID 1431564-(2-Chloroethoxy)benzaldehydeHCID 35514794-(3-Chloropropoxy)-benzaldehyde

Product 1

HCID 86754836HCID 86754836, compoundYield 34%

Procedure

A reaction was conducted in a manner similar to Referential Example 13 by using 1-(4-chlorophenyl)-2-imidazolidinone (Compound No. 2) in place of 1-(4-ethylphenyl)-2-imidazolidinone (Compound No. 1) and 4-(3-chloropropoxy)benzaldehyde in lieu of 4-(2-chloroethoxy)benzaldehyde, whereby the title compound was obtained in a yield of 34%.

Sources & evidence

ORD record
ord-f6355d032ae149bcb944db01b642ea10
Source dataset
uspto-grants-1999_11
Patent number
US05990139

Reaction notes

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