2-Bromo-1-chloro-4-nitrobenzene → HCID 18005084, compound

HRID 1603780Notes

Reaction equation

HRID 1603780 reaction equation
Br[C:2]1[CH:3]=[C:4]([N+:9]([O-:11])=[O:10])[CH:5]=[CH:6][C:7]=1[Cl:8].[CH3:12][C:13]1[CH:18]=[CH:17][N:16]=[CH:15][C:14]=1B(O)O>>[Cl:8][C:7]1[CH:6]=[CH:5][C:4]([N+:9]([O-:11])=[O:10])=[CH:3][C:2]=1[C:14]1[CH:15]=[N:16][CH:17]=[CH:18][C:13]=1[CH3:12]

Participants

3

Reactant 2

HCID 27355492-Bromo-1-chloro-4-nitrobenzeneHCID 27627114-Methylpyridine-3-Boronic Acid

Product 1

HCID 18005084HCID 18005084, compound

Procedure

The title compound was prepared by a Suzuki coupling of 3-bromo-4-chloronitrobenzene and 4-methyl-3-pyridylboronic acid. This gave (D61) (0.2 g, 33%).

Workup

  1. customThis gave (D61) (0.2 g, 33%)

Sources & evidence

ORD record
ord-dd7c56b5737e4fcd96c996af3275f92e
Source dataset
uspto-grants-1999_11
Patent number
US05990133

Reaction notes

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