HCID 53889921, compound → HCID 19606332, compound

Participants

Reaction Steps

A solution of 4-(4-phenylbutoxy)-2-fluorobenzyl alcohol (1.38 g, 5.03 mmol) in dichloromethane (50 ml) was added with pyridinium chlorochromate (1.63 g, 7.54 mmol), stirring at room temperature for 1 h. After that the reaction mixture was filtered on celite, washing with dichloromethane. After drying and removing the solvent, the resulting crude was purified by chromatography through a silica gel column, eluting with dichloromethane, thereby recovering 1.02 g of the title compound (74% yield).

Provenance & Evidence