HRID1604145

反应详情

EQUATION

反应方程式

HRID 1604145 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 3,5-dinitrobenzylalcohol (2.20 g, 11.1 mmol) in methanol (90 ml) and a Pd/C catalyst (10%, 100 mg) was hydrogenated in a Parr apparatus at 60 psi. The solution was filtered and the solvent was removed by evaporation. The crude product was used without purification in the next step.

WORKUP

后处理

  1. filtrationThe solution was filtered
  2. customthe solvent was removed by evaporation
  3. customThe crude product was used without purification in the next step