HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → HCID 19602324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | N-Ethylnaphthalene-2-carboxamide | HCID 12776824 | — |
| Product | HCID 19602324 | HCID 19602324 | 17% |
Reaction Steps
N-Ethyl-2-naphthalenecarboxamide was reacted with 2 eq TMSCl according to General Method C. The resulting reaction mixture was worked up in the usual manner, then purified by chromatography with 3:7 ethyl acetate/hexanes to afford 3.3 g of the desired compound as a white solid, a 17% yield. m.p. 132-136° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05994270 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-b14d41e1b9fc4779841481817bbe00d9 |
| Source note | uspto-grants-1999_11 |