Water → HCID 19602493, compound

Participants

Reaction Steps

A mixture of (3RS,5RS)-3-(N-Chloroacetylaminomethyl)-4-oxa-1-azabicyclo[3.2.0]heptan-7-one(260 mg), Sodium formate(97 mg) in Dimethyl sulfoxide(5 ml) was stirred at room temperature for 15 hrs, then 70° C. for 3days. The reaction mixture was poured into water, extracted with Chloroform and dried over Magnesium sulfate. The residue which obtained after removal of solvent in vacuo, was purified by flash chromatography (Ethyl acetate). The title compound was obtained as oil.

Provenance & Evidence