Phenyl chloroformate → HCID 22355085, compound

HRID 1604308Notes

Reaction equation

HRID 1604308 reaction equation
[NH2:1][CH:2]([CH3:15])[CH2:3][N:4]([CH3:14])[NH:5][C:6]1[CH:11]=[C:10]([Cl:12])[CH:9]=[C:8]([Cl:13])[CH:7]=1.Cl[C:17](OC1C=CC=CC=1)=[O:18]>>[Cl:13][C:8]1[CH:7]=[C:6]([N:5]2[C:17](=[O:18])[NH:1][CH:2]([CH3:15])[CH2:3][N:4]2[CH3:14])[CH:11]=[C:10]([Cl:12])[CH:9]=1

Participants

3

Reactant 2

HCID 15891Phenyl chloroformateHCID 22008584HCID 22008584, compound

Product 1

HCID 22355085HCID 22355085, compound

Procedure

Reacting 1-(2-aminopropyl)-1-methyl-2-(3,5-dichlorophenyl)hydrazine with phenyl chloroformate under presence of base to provide the title compound. m.p. 129-130° C.

Sources & evidence

ORD record
ord-3eb422e511814d478eaa013f326bea0a
Source dataset
uspto-grants-1999_11
Patent number
US05994355

Reaction notes

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