HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 17914893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 19603375 | HCID 19603375 | — |
| Product | HCID 17914893 | HCID 17914893 | 87.5% |
Reaction Steps
Trifluoroacetic acid (3.3 ml) was added to a solution of N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonylmethyl)-4-methylcarbamoylaniline (250 mg) in ice water bath and stirred for 20 hours at ambient temperature. The solvent was evaporated under reduced pressure. The residue was pulverized with diethyl ether to give N-(4-methylcarbamoylphenyl) glycine (125 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05994368 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-bdd1555dcdfb4856894c76631c03edf6 |
| Source note | uspto-grants-1999_11 |