HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 21540456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | HCID 15581953 | HCID 15581953 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21540456 | HCID 21540456 | — |
Reaction Steps
A mixture of 2-dimethylamino-2-(2-pyridyl)thioacetamide and 40% aqueous solution of cyclopropylamine is heated at reflux for 45 minutes. The mixture is cooled and water is added. The mixture is then extracted with chloroform and the extracts are dried, concentrated and the residue is recrystallized to give N-cyclopropyl-2-dimethylamino-2-(2-pyridyl)thioacetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03948892 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-4cdc894ed1f341d2928a5d9550e3b7fe |
| Source note | uspto-grants-1976_04 |