HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → p-Chloromethylphenylacetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-(Chloromethyl)phenylacetic acid | HCID 10313419 | — |
| Product | p-Chloromethylphenylacetyl chloride | HCID 20380233 | — |
Reaction Steps
A mixture of 1 g of p-chloromethylphenylacetic acid and 6 ml of thionyl chloride is stirred at room temperature for 25 hours after which the excess thionyl chloride is removed under vacuum to yield p-chloromethylphenylacetyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03948904 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-bc07c8032e5d45218ae2f774098fd947 |
| Source note | uspto-grants-1976_04 |