Cyanamide → HCID 12272865, compound

HRID 1604931Notes

Reaction equation

HRID 1604931 reaction equation
Cl.[C:2]([CH2:4][C:5](=[NH:10])[O:6][CH2:7][CH2:8][CH3:9])#[N:3].[N:11]#[C:12]N>>[C:12]([N:10]=[C:5]([O:6][CH2:7][CH2:8][CH3:9])[CH2:4][C:2]#[N:3])#[N:11]

Participants

3

Reactant 2

HCID 9864CyanamideHCID 88841783HCID 88841783, compound

Product 1

HCID 12272865HCID 12272865, compoundYield 72.2%

Procedure

3.25 g of n-propyl cyanoacetimidate hydrochloride and 1.26 g of cyanamide were treated with the same manner as in Example 1 and 2.18 g of oily n-propyl N-cyanocyanoacetimidate was obtained (yield 72.1%). The structure of this compound was confirmed by IR and NMR. Analysis calculated for C7H9N3O C 55.62, H 6.00, N 27.80, found C 54.80, H 6.27, N 27.13.

Sources & evidence

ORD record
ord-64d38d0451ec4c719cf9df2ea5b3f078
Source dataset
uspto-grants-1976_04
Patent number
US03948915

Reaction notes

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