Allyl bromide → 2-(Nitromethylidene)-1-(prop-2-en-1-yl)-1,3-diazepane

HRID 1605011Notes

Reaction equation

[N+:1]([CH:4]=[C:5]1[NH:11][CH2:10][CH2:9][CH2:8][CH2:7][NH:6]1)([O-:3])=[O:2].[CH2:12](Br)[CH:13]=[CH2:14]>>[N+:1]([CH:4]=[C:5]1[NH:6][CH2:7][CH2:8][CH2:9][CH2:10][N:11]1[CH2:14][CH:13]=[CH2:12])([O-:3])=[O:2]

Participants

Reactant 2

HCID 7841Allyl bromide

HCID 116583251H-1,3-Diazepine, hexahydro-2-(nitromethylene)-

Product 1

HCID 706385112-(Nitromethylidene)-1-(prop-2-en-1-yl)-1,3-diazepane

Procedure

Method B, reacting hexahydro- 2-(nitromethylene)-1H-1,3-diazepine with allyl bromide. Melting point: 82° - 83° .

Sources & evidence

ORD record: ord-da45f8600fab41eea76b7130955493b8
Source dataset: uspto-grants-1976_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03948934

Reaction notes

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