Acetic Anhydride → HCID 21548934, compound

HRID 1605051Notes

Reaction equation

HRID 1605051 reaction equation
[CH:1]1[C:14]2[CH2:13][C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[O:6][C:5]=2[CH:4]=[CH:3][C:2]=1[CH:15](C)[CH2:16][OH:17].[C:19](OC(=O)C)(=[O:21])[CH3:20]>N1C=CC=CC=1>[C:19]([O:17][CH2:16][CH2:15][C:2]1[CH:3]=[CH:4][C:5]2[O:6][C:7]3[C:12](=[CH:11][CH:10]=[CH:9][CH:8]=3)[CH2:13][C:14]=2[CH:1]=1)(=[O:21])[CH3:20]

Participants

4

Reactant 2

HCID 7918Acetic AnhydrideHCID 21548938HCID 21548938, compound

Product 1

HCID 21548934HCID 21548934, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

One gram of 2-(2-xanthenyl)-propanol is allowed to stand for 24 hours in 5 ml. of pyridine and 5 ml. of acetic anhydride. The mixture is concentrated, worked up as usual, and the product is 2-(2-xanthenyl)-propyl acetate, m.p. 62°-64°.

Workup

  1. concentrationThe mixture is concentrated

Sources & evidence

ORD record
ord-30712e878f3f4ff2b742d5c04d54e32c
Source dataset
uspto-grants-1976_04
Patent number
US03948949

Reaction notes

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