Boron tribromide → HCID 21549142, compound

HRID 1605114Notes

Reaction equation

[F:1][C:2]1([F:15])[C:4]([CH3:6])([CH3:5])[CH:3]1[C:7]1[CH:12]=[CH:11][C:10]([O:13]C)=[CH:9][CH:8]=1.B(Br)(Br)Br>>[F:1][C:2]1([F:15])[C:4]([CH3:6])([CH3:5])[CH:3]1[C:7]1[CH:8]=[CH:9][C:10]([OH:13])=[CH:11][CH:12]=1

Participants

Reactant 2

HCID 25134Boron tribromide

HCID 21549184HCID 21549184, compound

Product 1

HCID 21549142HCID 21549142, compound

Procedure

p-(2,2-Difluoro-3,3-dimethylcyclopropyl)phenol was prepared from 31.8 g. of p-(2,2-difluoro-3,3-dimethylcyclopropyl)anisole and 25 g. of boron tribromide according to the procedure described above in Example 1, part (c). The product was used directly in the following reaction without further purification.

Workup

customThe product was used directly in the following reaction without further purification

Sources & evidence

ORD record: ord-416eaf5bef73480393f5c5c98fe7ee94
Source dataset: uspto-grants-1976_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03948973

Reaction notes

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