Boron tribromide → 52178-86-6
Reaction equation
[F:1][C:2]1([F:13])[CH2:4][CH:3]1[C:5]1[CH:10]=[CH:9][C:8]([O:11]C)=[CH:7][CH:6]=1.B(Br)(Br)Br>>[F:1][C:2]1([F:13])[CH2:4][CH:3]1[C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1Participants
3
Procedure
p-(2,2-Difluorocyclopropyl)phenol was prepared from 120 g. of p-(2,2-difluorocyclopropyl)anisole and 81 g. of boron tribromide according to the procedure described above in Example 1, part (c), affording 72 g. of oil used directly in the following reaction.
Workup
- customaffording 72 g
- customof oil used directly in the following reaction
Sources & evidence
- ORD record
- ord-9760bec5e0814e4fb5ceb31c1e14c843
- Source dataset
- uspto-grants-1976_04
- Patent number
- US03948973
Reaction notes
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