HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanethiol → 7-Methylthio-3,7-dimethyloctan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanethiol | HCID 878 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Citronellol | HCID 8842 | — |
| Product | 7-Methylthio-3,7-dimethyloctan-1-ol | HCID 21549353 | — |
Reaction Steps
Twenty grams of citronellol, 2 g. of p-toluenesulfonic acid and 9 g. of methyl mercaptan are reacted as described in Example 44 except that a temperature of 140° is used instead of 220°, to give 7-methylthio-3,7-dimethyloctan-1-ol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03948996 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-e7ab736c8a9941629012e6c775537a64 |
| Source note | uspto-grants-1976_04 |