Hydrochloric Acid → HCID 20492236, compound

Participants

Reaction Steps

27.6 G (0.125 mole) of (4-hydroxy-3-methyl-5-tert. butylbenzyl) dimethylamine, 30.5 g (0.05 mole) of malonic acid distearyl ester, and 0.5 g of sodium methylate were refluxed in 100 cc of absolute toluene for 21/2 hours while a current of nitrogen was passed through the reaction mixture. After cooling, the reaction mixture was diluted with methylene chloride, shaken out with 2N hydrochloric acid and water, and evaporated to dryness. The residue was slurried in methanol, filtered, and washed.

Provenance & Evidence