HCID 21546866, compound → HCID 54504572, compound

HRID 1605556Notes

Reaction equation

HRID 1605556 reaction equation
C([NH:8]C1C=C(C=C(S(Cl)(=O)=O)C=1C1C=CC=CC=1)C(O)=O)C1C=CC=CC=1.[CH2:28]([O:32][C:33]1[CH:34]=[C:35]([CH:39]=[C:40]([S:48](Cl)(=[O:50])=[O:49])[C:41]=1[C:42]1[CH:47]=[CH:46][CH:45]=[CH:44][CH:43]=1)[C:36]([OH:38])=[O:37])[CH2:29][CH2:30][CH3:31]>>[CH2:28]([O:32][C:33]1[CH:34]=[C:35]([CH:39]=[C:40]([S:48](=[O:50])(=[O:49])[NH2:8])[C:41]=1[C:42]1[CH:47]=[CH:46][CH:45]=[CH:44][CH:43]=1)[C:36]([OH:38])=[O:37])[CH2:29][CH2:30][CH3:31]

Participants

3

Reactant 2

HCID 21546866HCID 21546866, compoundHCID 21546891HCID 21546891, compound

Product 1

HCID 54504572HCID 54504572, compound

Procedure

By replacing in Example 1, step G, 3-benzylamino-5-chlorosulfonyl-4-phenylbenzoic acid with 3-n-butoxy-5-chlorosulfonyl-4-phenylbenzoic acid, and following the procedure described, 3-n-butoxy-4-phenyl-5-sulfamylbenzoic acid is obtained crystallizing with 0.25 mole of water with a melting point of 129°-131° C.

Sources & evidence

ORD record
ord-ce6f4a36277e4839ae4da1cf5173d0fa
Source dataset
uspto-grants-1976_04
Patent number
US03950380

Reaction notes

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