HCID 21546866, compound → HCID 21546858, compound

HRID 1605569Notes

Reaction equation

HRID 1605569 reaction equation
C([NH:8]C1C=C(C=C(S(Cl)(=O)=O)C=1C1C=CC=CC=1)C(O)=O)C1C=CC=CC=1.[CH2:28]([S:31][C:32]1[CH:33]=[C:34]([CH:38]=[C:39]([S:47](Cl)(=[O:49])=[O:48])[C:40]=1[C:41]1[CH:46]=[CH:45][CH:44]=[CH:43][CH:42]=1)[C:35]([OH:37])=[O:36])[CH:29]=[CH2:30]>>[CH2:28]([S:31][C:32]1[CH:33]=[C:34]([CH:38]=[C:39]([S:47](=[O:49])(=[O:48])[NH2:8])[C:40]=1[C:41]1[CH:46]=[CH:45][CH:44]=[CH:43][CH:42]=1)[C:35]([OH:37])=[O:36])[CH:29]=[CH2:30]

Participants

3

Reactant 2

HCID 21546866HCID 21546866, compoundHCID 21546901HCID 21546901, compound

Product 1

HCID 21546858HCID 21546858, compound

Procedure

By replacing in Example 1, step G, 3-benzylamino-5-chlorosulfonyl-4-phenylbenzoic acid with 3-allylthio-5-chlorosulfonyl-4-phenylbenzoic acid, and following the procedure described, 3-allylthio-4-phenyl-5-sulfamylbenzoic acid is obtained as a hydrate with a melting point of 78°-81° C.

Sources & evidence

ORD record
ord-e9c6cd31f8bf4419b8b38d14a47c9f79
Source dataset
uspto-grants-1976_04
Patent number
US03950380

Reaction notes

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