HRID1605571

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=C(O)c1cc(NCc2ccccc2)c(-c2ccccc2)c(S(=O)(=O)Cl)c1

HCID21546866

未命名化合物

结构：CC=CCSc1cc(C(=O)O)cc(S(=O)(=O)Cl)c1-c1ccccc1

HCID54083085

未命名化合物

PRODUCTS

生成物

结构：CC=CCSc1cc(C(=O)O)cc(S(N)(=O)=O)c1-c1ccccc1

HCID54063665

未命名化合物

PROCEDURE

实验过程

By replacing in Example 1, step G, 3-benzylamino-5-chlorosulfonyl-4-phenylbenzoic acid with 5-chlorosulfonyl-3-crotylthio-4-phenylbenzoic acid, and following the procedure described, 3-crotylthio-4-phenyl-5-sulfamylbenzoic acid is obtained crystallizing with 0.5 mole of ethanol with a melting point of 89°-91° C.