HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 3-Allylamino-4-phenyl-5-sulfamylbenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 3-Amino-5-nitro-4-phenylbenzoic acid | HCID 12408769 | — |
| Reactant | 3-Amino-4-phenyl-5-sulfamylbenzoic acid | HCID 21546841 | — |
| Product | 3-Allylamino-4-phenyl-5-sulfamylbenzoic acid | HCID 21546828 | — |
Reaction Steps
By replacing in Example 1, step D, 3-amino-5-nitro-4-phenylbenzoic acid and benzyl bromide with equimolar amounts of 3-amino-4-phenyl-5-sulfamylbenzoic acid and allyl bromide respectively, and following the procedure described, 3-allylamino-4-phenyl-5-sulfamylbenzoic acid is obtained with a melting point of 169°-172.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03950380 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-627eb7b77fe24a48bcf4845430ec63de |
| Source note | uspto-grants-1976_04 |