HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 20319174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 20318970 | HCID 20318970 | — |
| Product | HCID 20319174 | HCID 20319174 | — |
Reaction Steps
1.53 gm of 2-amino-3-bromo-N,N-diethyl-5-methyl-benzylamine hydrochloride were dissolved in 50 ml of acetic acid anhydride at 75°C. The solution was evaporated to dryness in vacuo, and the residue was recrystallized from ethanol, yielding 2-acetamino-3-bromo-N,N-diethyl-5-methyl-benzylamine hydrochloride, m.p. 170°-172°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03950393 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-2d8e44de94df477aa2614c04d027a93c |
| Source note | uspto-grants-1976_04 |