HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 2-Amino-3-bromo-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 2-Amino-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine | HCID 20319198 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Amino-3-bromo-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine | HCID 20319233 | — |
Reaction Steps
2-Amino-3-bromo-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine was prepared from 2-amino-N-cyclohexyl-N-ethyl-5-methoxy-benzylamine and bromine analogous to Example 9. Proof of structure by IR-, UV- and NMR-spectra. IR-spectrum (methylenechloride):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03950393 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-cdda6805ab864a4cb313a3552dba3bf1 |
| Source note | uspto-grants-1976_04 |