HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Tert-octylphenol → 4-Tert-octylcatechol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Tert-octylphenol | HCID 8814 | — |
| Reactant | Perpropionic acid | HCID 65136 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 4-Tert-octylcatechol | HCID 70828 | 58% |
Reaction Steps
The procedure of Example 9 was repeated, except 10.4g (0.1 mol) of perisobutyric acid in the form of about 20 weight% acetone solution was added over 30 minutes in place of perpropionic acid. Consequently, the conversion of para-tert.-octyl phenol was 13.2%, 4-tert.-octyl pyrocatechol was formed in a yield of 58% based on the converted octyl phenol and the conversion of perisobutyric acid was 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03950437 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-68b802726e934ca9a2f2937935a17169 |
| Source note | uspto-grants-1976_04 |