HuagongsheHuagongshe Chemistry Print Report · For research reference only
(E)-3-Methoxy-2-butenoic acid methyl ester → HCID 68135585, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (E)-3-Methoxy-2-butenoic acid methyl ester | HCID 5357209 | — |
| Reactant | HCID 22718775 | HCID 22718775 | — |
| Product | HCID 68135585 | HCID 68135585 | 28% |
Reaction Steps
(E)-4-(4-cycloheptyl-phenyl)-3-pentene-2-one was prepared analogous to Example 52 from 4'-cycloheptyl-acetophenone (b.p. 120°-125°C at 0.03 mm Hg) and methyl (E)-3-methoxy-crotonate with a yield of 28% of theory. B.p. 132°-135°C at 0.1 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03950427 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-9c910111c7e2407986d687ed590bdc40 |
| Source note | uspto-grants-1976_04 |