HCID 54216389, compound → HCID 21547098, compound

HRID 1605672Notes

Reaction equation

HRID 1605672 reaction equation
[CH:1]1([C:7]2[CH:12]=[CH:11][C:10]([C:13]([CH2:18][CH3:19])=[CH:14][C:15](=[O:17])[CH3:16])=[CH:9][CH:8]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C1(C2C=CC(/C(/CC)=C/C(=O)C)=CC=2)CCCCC1>>[CH:1]1([C:7]2[CH:8]=[CH:9][C:10]([CH:13]([CH2:18][CH3:19])[CH2:14][C:15](=[O:17])[CH3:16])=[CH:11][CH:12]=2)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1

Participants

3

Reactant 2

HCID 54216389HCID 54216389, compound2×HCID 68133940HCID 68133940, compound

Product 1

HCID 21547098HCID 21547098, compoundYield 86%

Procedure

4-(4-Cyclohexyl-phenyl)-2-hexanone was prepared analogous to Example 66 from the mixture of isomers of 4-(4-cyclohexylphenyl)-3-hexene-2-one and 4-(4-cyclohexyl-phenyl)-3-hexene-2-one and 4-(4-cyclohexyl-phenyl)-4-hexene-2-one obtained in Example 56. Yield: 86% of theory. B.p. 137°-142°C at 0.1 mm Hg.

Sources & evidence

ORD record
ord-afe2843fb1fe4b9e95f553c2af219e08
Source dataset
uspto-grants-1976_04
Patent number
US03950427

Reaction notes

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