HuagongsheHuagongshe Chemistry Print Report · For research reference only
beta-Aminobeta-ethoxyacrylic acid ethyl ester → 3-Amino-1-(3-nitrobenzyl)-pyrazol-5-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | beta-Aminobeta-ethoxyacrylic acid ethyl ester | HCID 278451 | — |
| Reactant | (3-Nitrobenzyl)hydrazine | HCID 20511322 | — |
| Product | 3-Amino-1-(3-nitrobenzyl)-pyrazol-5-one | HCID 20367193 | — |
Reaction Steps
17.5 g of β-amino-β-ethoxyacrylic acid ethyl ester and 16.7 g of 3-nitrobenzylhydrazine, analogously to the procedure described in Example 1 yield 12.3 g of the compound identified above as yellow crystals of melting point 163°, corresponding to 52% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03950528 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-db35f9cf917f412591e521a20e74fd49 |
| Source note | uspto-grants-1976_04 |