2-Chlorobenzylhydrazine → HCID 20367316, compound

HRID 1605737Notes

Reaction equation

HRID 1605737 reaction equation
C([O:3][C:4](=O)[C:5](OCC)=[CH:6][NH2:7])C.[Cl:12][C:13]1[CH:21]=[CH:20][CH:19]=[CH:18][C:14]=1[CH2:15][NH:16][NH2:17]>>[NH2:7][C:6]1[NH:17][N:16]([CH2:15][C:14]2[CH:18]=[CH:19][CH:20]=[CH:21][C:13]=2[Cl:12])[C:4](=[O:3])[CH:5]=1

Participants

3

Reactant 2

HCID 4170642-ChlorobenzylhydrazineHCID 86733242HCID 86733242, compound

Product 1

HCID 20367316HCID 20367316, compoundYield 40%

Procedure

35 g of β-amino--ethoxyacrylic acid ethyl ester and 32 g of 2-chlorobenzylhydrazine when reacted as described in Example 45 yield 17.5 g of the compound identified above as colorless crystals of melting point 153°. (Yield: 40% of theory)

Sources & evidence

ORD record
ord-f1f2abed138c476b963969ea27f82ece
Source dataset
uspto-grants-1976_04
Patent number
US03950528

Reaction notes

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