HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 12450695, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2(5H)-Furanone, 5-hydroxy-3,4-dimethyl- | HCID 2752890 | — |
| Product | HCID 12450695 | HCID 12450695 | — |
Reaction Steps
A mixture of 6.6g of 2-hydroxy-3,4-dimethyl-5-oxo-2,5-dihydrofuran and 10 ml of thionyl chloride was stirred for 2 hours at room temperature. By concentrating the reaction mixture under reduced pressure, 7.5g of light-yellowish oily 2-chloro-3,4-dimethyl-5-oxo-2,5-dihydrofuran was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03951954 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-50fe49a96bdc4898b4393489f015e892 |
| Source note | uspto-grants-1976_04 |