Methyl iodide → HCID 20369327, compound

HRID 1605857Notes

Reaction equation

HRID 1605857 reaction equation
[C:1]([NH:4][C:5]1[CH:13]=[CH:12][C:8]([C:9](=[S:11])[NH2:10])=[CH:7][CH:6]=1)(=[O:3])[CH3:2].[CH3:14][I:15]>CC(C)=O>[IH:15].[C:1]([NH:4][C:5]1[CH:13]=[CH:12][C:8]([C:9]([S:11][CH3:14])=[NH:10])=[CH:7][CH:6]=1)(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 3000565N-(4-carbamothioylphenyl)acetamide

Product 1

HCID 20369327HCID 20369327, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

To a mixture of 2.7 g. (0.014 mole) of p-acetamidobenzthioamide in 100 ml. of acetone is added 2.6 ml. of methyl iodide, and the resulting reaction mixture allowed to stir at room temperature overnight. The intermediate product is filtered and dried, 4.4 g., m.p. 216°-217° C.

Workup

  1. additionTo a mixture of 2.7 g
  2. filtrationThe intermediate product is filtered
  3. customdried

Sources & evidence

ORD record
ord-ace5e34230404d4687c42b6ca715d72c
Source dataset
uspto-grants-1976_04
Patent number
US03951952

Reaction notes

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