HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 12521677, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 20355326 | HCID 20355326 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12521677 | HCID 12521677 | — |
Reaction Steps
A solution of 6-methoxy-10-(methylthio)-4H-thieno[3,4-b][1,5]benzodiazepine in excess N-methylpiperazine and glacial acetic acid is heated at reflux for 2 days. The solution is poured into water and the product is collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03951981 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-98a21c2daf1f4dc7a1d0561221de9bc0 |
| Source note | uspto-grants-1976_04 |